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Jun 08, 2014 The ball milling (BM) pretreatment was performed according to the method reported by Silva et al. . Raw materials (2-mm particle size, dried in vacuo at 40 C) were treated using the Pulverisette 5 planetary ball mill (Fritsch, Germany). The sample (20 g) was milled at 250 rpm in a 500-mL milling cup with 25 spheres (ψ = 20 mm). Milling was ...
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